Nnyocha na usoro njikọ nke bis (fluorosulfonyl) amide

Na gburugburu ebe na-emebi emebi nke ukwuu, nleba anya nleba anya n'ịntanetị na-aghọ ụzọ nyocha dị irè.

Enwere ike iji lithium bis (fluorosulfonyl) amide (LiFSI) dị ka ihe mgbakwunye maka batrị batrị lithium-ion, yana uru dị ka njupụta ume dị elu, nkwụsi ike ọkụ, na nchekwa.Ọchịchọ n'ọdịnihu na-apụta ìhè karị, na-eme ka ọ bụrụ ebe na-ekpo ọkụ na nyocha ụlọ ọrụ ike ọhụrụ.

Usoro njikọ nke LiFSI gụnyere fluoridation.Dichlorosulfonyl amide na-emeghachi omume na HF, ebe Cl dị n'ime ihe ahụ molekụla na-anọchi F, na-emepụta bis (fluorosulfonyl) amide.N'oge usoro a, a na-emepụta ngwaahịa ndị dị n'etiti nke na-edochibeghị nke ọma.Ọnọdụ mmeghachi omume siri ike: HF na-emebi emebi na oke egbu egbu;mmeghachi omume na-eme n'okpuru okpomọkụ dị elu na nrụgide, na-eme ka usoro ahụ dị ize ndụ.

Ka ọ dị ugbu a, ọtụtụ nyocha gbasara mmeghachi omume a na-elekwasị anya n'ịchọta ọnọdụ mmeghachi omume kacha mma iji bulie mkpụrụ ngwaahịa.Naanị usoro nchọpụta na-anọghị n'ịntanetị dị maka ihe niile bụ F nuclear magnet resonance (NMR) spectrum.Usoro nchọpụta ahụ dị oke mgbagwoju anya, na-ewe oge ma dị ize ndụ.N'ime mmeghachi omume ngbanwe, nke na-adịru ọtụtụ awa, a ga-ahapụrịrị nrụgide ma were nlele kwa nkeji 10-30 ọ bụla.A na-eji F NMR nwalee ihe nlele ndị a iji chọpụta ọdịnaya nke ngwaahịa etiti na akụrụngwa.Usoro mmepe ahụ dị ogologo, nlele anya dị mgbagwoju anya, na usoro nlele ahụ na-emetụtakwa mmeghachi omume ahụ, na-eme ka data ule na-enweghị atụ.

Agbanyeghị, teknụzụ nleba anya n'ịntanetị nwere ike idozi oke nke nlekota n'ịntanetị.N'ime njikarịcha usoro, enwere ike iji spectroscopy n'ịntanetị iji nyochaa mkpokọta n'ime ọnọdụ nke reactants, ngwaahịa etiti, na ngwaahịa.Ihe nyocha nke imikpu na-eru ozugbo n'okpuru mmiri mmiri n'ime kettle mmeghachi omume.Nyocha ahụ nwere ike iguzogide corrosion sitere na ihe ndị dị ka HF, hydrochloric acid, na chlorosulfonic acid, ma nwee ike ịnagide okpomọkụ ruo 200 Celsius C na nrụgide 15 MPa.The ekpe eserese na-egosi online nlekota nke reactants na etiti ngwaahịa n'okpuru asaa usoro parameters.N'okpuru oke 7, a na-eri ngwa ngwa ngwa ngwa, na mmeghachi omume na-emecha nke mbụ, na-eme ka ọ bụrụ ọnọdụ mmeghachi omume kacha mma.